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Synthesis of Amidomethyltrifluoroborates and Their Use in Cross-Coupling Reactions

Author(s): Molander, GA (Molander, Gary A.); Hiebel, MA (Hiebel, Marie-Aude) Addresses: [Molander, Gary A.; Hiebel, Marie-Aude] Univ Penn, Dept Chem, Roy & Diana Vagelos Labs, Philadelphia, PA 19104 USA. Source: ORGANIC LETTERS, 12 (21): 4876-4879 NOV 5 2010

Amidomethyltrifluoroborates were successfully synthesized in a one-pot fashion and used in cross-coupling reactions with a wide variety of aryl and heteroaryl chlorides.

Author(s):  Molander, GA (Molander, Gary A.); Hiebel, MA (Hiebel, Marie-Aude)
Addresses:  [Molander, Gary A.; Hiebel, Marie-Aude] Univ Penn, Dept Chem, Roy & Diana Vagelos Labs, Philadelphia, PA 19104 USA.
Source:  ORGANIC LETTERS, 12 (21): 4876-4879 NOV 5 2010
DOI: 10.1021/ol102039c
Publisher:  AMER CHEMICAL SOC
Funding Agency:  This research was supported by a National Priorities Research Program (NPRP) grant from the Qatar National Research Fund (Grant no. 08-035-1-008) and the NIH (R01 GM-081376). We thank Frontier Scientific for a generous gift of Pd(OAc)2. Dr. Rakesh Kohli (University of Pennsylvania) is acknowledged for obtaining HRMS data. 
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